HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 9930032, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 2-Bromoethyl methyl ether | HCID 80972 | — |
| Reactant | HCID 17786842 | HCID 17786842 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 9930032 | HCID 9930032 | — |
Reaction Steps
0.491 g (1.5 mmol) of N-[2,2-dimethyl-6-hydroxychroman-4-yl]-N-(1-propyl)ethanesulfonamide (Example 22b) was reacted with NaH and 2-methoxyethyl bromide in DMA. 0.27 g of the title compound was obtained from petroleum ether, m.p. 78-80° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06177449B1 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-64ff4a00b59f490a9b8701d85f7f4346 |
| Source note | uspto-grants-2001_01 |