HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Anisoyl chloride → HCID 21264403, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Anisoyl chloride | HCID 74374 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | HCID 2739390 | HCID 2739390 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 21264403 | HCID 21264403 | — |
Reaction Steps
4-(4-Trifluoromethylphenyl)-4,5,6,7-tetrahydro-thieno[3,2-c]pyridine (100 mg, 0.35 mmol) was dissolved in dichloromethane (1 mL) and diisopropylethylamine (0.5 mL) was added. To this solution m-anisoyl chloride (50 μL, 0.35 mmol) was added. The mixture was shaken overnight and evaporated to afford the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06177443B1 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-466aacee0a1b471c854e83464e03553d |
| Source note | uspto-grants-2001_01 |