HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridinium hydrochloride → 5-Chloro-4-[5-chloro-2-(trifluoromethyl)phenyl]pyridin-2(1H)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridinium hydrochloride | HCID 21584435 | — |
| Reactant | 5-Chloro-4-[5-chloro-2-(trifluoromethyl)phenyl]-2-methoxypyridine | HCID 117605620 | — |
| Product | 5-Chloro-4-[5-chloro-2-(trifluoromethyl)phenyl]pyridin-2(1H)-one | HCID 117605078 | — |
Reaction Steps
193 mg (purity 93%, 0.56 mmol) of 5-chloro-4-[5-chloro-2-(trifluoromethyl)phenyl]-2-methoxypyridine and pyridinium hydrochloride were reacted according to General Method 3A. Yield: 123 mg (72% of theory)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09434690B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-b35b67511b614215be80aa4dd7ee22ee |
| Source note | uspto-grants-2016_09 |