HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrobenzaldehyde → HCID 21264431, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrobenzaldehyde | HCID 541 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Thiopheneethanamine | HCID 116521 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21264431 | HCID 21264431 | 76% |
Reaction Steps
2-(2-Thienyl)-ethylamine (5 g, 39.4 mmol), 4-nitrobenzaldehyde and triethylamine (10 ml) were dissolved in ethanol (100 ml). The reaction mixture was stirred at room temperature for 48 hours. The solid formed was filtered and dried to afford 7.75 g (76%) (4-nitrobenzylidene)-(2-thiophen-2-yl-ethyl)-amine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06177443B1 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-fcc09dbcfab045de933e252b3ca7ee13 |
| Source note | uspto-grants-2001_01 |