HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → HCID 178518915, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | 2-(4-Fluorobenzylcarbonyl)benzoic acid | HCID 13799982 | — |
| Product | HCID 178518915 | HCID 178518915 | — |
Reaction Steps
A 3 M ethanolic solution of hydrazine (20 ml, 60 mmol) is added to 2-(4-fluorobenzyl carbonyl)benzoic acid (5.5 g, 20 mmol), and the mixture is stirred at room temperature for 5 hours. Precipitation gives 4-(4-fluorobenzyl)-1-hydroxy-phthalazine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06180629B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-41bd89e2715e4c33a2a322bab750b0bd |
| Source note | uspto-grants-2001_01 |