HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 21262529, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | HCID 21262524 | HCID 21262524 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 21262529 | HCID 21262529 | — |
Reaction Steps
The product of part C, 2-amino-5,8-difluoro-4-(2-pyridyl)-(2H)-1-phthalazinone (0.01 mol) is stirred overnight with benzoylchloride in dichloromethane at room temperature. The product is recrystallized to yield the title compound (R1=benzyl, Y1=—NH—C(O), R2=2-pyridyl, A=benzene, R3=F, F, m=2, p=0).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06180629B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-594a0734281f48498e20601dd875fccf |
| Source note | uspto-grants-2001_01 |