HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 567790Generated: October 26, 2026
Acetone → 2-{[4-(3-methoxylpropoxy)-3-methylpyridin-2-yl]methylsulfinyl}-1H-benzimidazole Sodium Salt Acetone
https://huagongshe.com/reaction/567790
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | (S)-Rabeprazole sodium | HCID 9821387 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 2-{[4-(3-methoxylpropoxy)-3-methylpyridin-2-yl]methylsulfinyl}-1H-benzimidazole Sodium Salt Acetone | HCID 131722286 | 146.3% |
Reaction Steps
2-{[4-(3-Methoxypropoxy)-3-methylpyridin-2-yl]methylsulfinyl}-1H-benzimidazole sodium salt (7.0 g) was dissolved in ethyl acetate (3 ml), and acetone (3 ml) was added thereto, and the mixture was stirred at 5° C. for 12 hours. The precipitated white crystals were filtered and dried to give the title compound (5.9 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06180652B2 |
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| Source dataset | uspto-grants-2001_01 |
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| ORD ID | ord-a5aa635aca124141ba4b7e33ee40e767 |
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| Source note | uspto-grants-2001_01 |
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