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HRID567792

反应详情

EQUATION

反应方程式

HRID 567792 的结构方程式

REACTANTS

反应物

1
结构：CC(C)=O.COCCCOc1ccnc(CS(=O)c2nc3ccccc3[nH]2)c1C.[Na]
HCID131722286

未命名化合物

PRODUCTS

生成物

1
结构：COCCCOc1ccnc(CS(=O)c2nc3ccccc3[nH]2)c1C.[Na]
HCID9821387

未命名化合物

收率 101.4%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

After the acetone complex (10.0 g) obtained in Example 7 was dissolved in distilled water (20 ml), it was frozen in a dry ice/methanol bath. It was then lyophilized for 48 hours to give the amorphous title compound (8.8 g) (yield: quantitative).

WORKUP

后处理

  1. temperatureit was frozen in a dry ice/methanol bath