O-Phenylenediamine → HCID 21263225, compound

HRID 568021Notes

Reaction equation

HRID 568021 reaction equation
[N:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][C:9]=2[S:11](Cl)(=[O:13])=[O:12])[CH:4]=[CH:3][CH:2]=1.[C:15]1([NH2:22])[CH:20]=[CH:19][CH:18]=[CH:17][C:16]=1[NH2:21]>>[N:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][C:9]=2[S:11]([NH:21][C:16]2[CH:17]=[CH:18][CH:19]=[CH:20][C:15]=2[NH2:22])(=[O:13])=[O:12])[CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 7243O-PhenylenediamineHCID 292208-Quinolinesulfonyl chloride

Product 1

HCID 21263225HCID 21263225, compound

Procedure

The sulfonamide was synthesized from 8-quinolinyl sulfonyl chloride(0.01 mol) and o-phenylene diamine(0.01 mol) by general Method C. It was purified by recrystallization from EtOH(0.82 g, 27%). EI-MS m/z 300 (M+H)+.

Workup

  1. customIt was purified by recrystallization from EtOH(0.82 g, 27%)

Sources & evidence

ORD record
ord-51afdb00669c407c82084761637f8840
Source dataset
uspto-grants-2001_01
Patent number
US06180675B2

Reaction notes

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