HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Phenylenediamine → HCID 21263225, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Phenylenediamine | HCID 7243 | — |
| Reactant | 8-Quinolinesulfonyl chloride | HCID 29220 | — |
| Product | HCID 21263225 | HCID 21263225 | — |
Reaction Steps
The sulfonamide was synthesized from 8-quinolinyl sulfonyl chloride(0.01 mol) and o-phenylene diamine(0.01 mol) by general Method C. It was purified by recrystallization from EtOH(0.82 g, 27%). EI-MS m/z 300 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06180675B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-51afdb00669c407c82084761637f8840 |
| Source note | uspto-grants-2001_01 |