HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Phenylenediamine → 2-(Benzylsulfonylamino)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Phenylenediamine | HCID 7243 | — |
| Reactant | Phenylmethanesulfonyl chloride | HCID 74740 | — |
| Product | 2-(Benzylsulfonylamino)aniline | HCID 16778443 | — |
Reaction Steps
The sulfonamide was synthesized from benzylsulfonyl chloride(0.01 mol) and o-phenylene diamine(0.01 mol) by general Method C. It was purified by recrystallization from EtOH(0.87g, 33%). EI-MS m/z 263(M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06180675B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-84e63cb069224b47bd25fa740552c59a |
| Source note | uspto-grants-2001_01 |