HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 70219254, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | 4-Methylbenzoyl Chloride | HCID 13405 | — |
| Reactant | 4-Amino-m-cresol | HCID 17819 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 70219254 | HCID 70219254 | 12% |
Reaction Steps
4-Methylbenzoyl chloride was added to a DMF solution of a mixture of 4-amino-3-methylphenol and triethylamine, and stirred at room temperature for 30 minutes. The relative amount of each compound used, and the purification of the product. is described in Production Example 4. Thus was obtained the intended product, 4-hydroxy-2-methylphenyl-4-methylbenzamide (yield: 12%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06180844B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-6313b33ec239490388b1ad5064ffb9a9 |
| Source note | uspto-grants-2001_01 |