HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Acetate → HCID 178506542, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | 2-phenyl-1H-imidazole-1-propanamine | HCID 13588911 | — |
| Reactant | 2-Methylthiobenz(cd)indole hydriodide | HCID 20150650 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178506542 | HCID 178506542 | — |
Reaction Steps
A mixture of 4.0 g of 3-(2-phenyl-1H-imidazol-1-yl)propanamine, 6.5 g of 2-(methylthio)benz[cd]indole hydroiodide, 1.8 g of sodium acetate and 250 ml of ethanol was reacted as described in Example 11. The crude product was recrystallized from a mixture of ethanol and isopropanol giving 3.8 g of the desired product, mp 153° C.-155° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04728663 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-94426a4fab0e4a74b7e098f23b6c070b |
| Source note | uspto-grants-1988_03 |