HRID568489

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID517045

Sodium Acetate

C2H3NaO2

HCID3152105

3-(2-methyl-1H-imidazol-1-yl)propan-1-amine

C7H13N3

HCID20150650

未命名化合物

PRODUCTS

生成物

HCID178432904

未命名化合物

收率 15.8%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

A mixture of 2.1 g of 3-(2-methyl-1H-imidazol-1-yl)propanamine, 5.0 g of 2-(methylthio)benz[cd]indole hydroiodide, 1.4 g of sodium acetate and 250 ml of ethanol was reacted as described in Example 13, giving 1.0 g of the desired product, mp 153°-155° C.

WORKUP

后处理

customwas reacted