HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Acetate → HCID 178432904, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | 3-(2-methyl-1H-imidazol-1-yl)propan-1-amine | HCID 3152105 | — |
| Reactant | 2-Methylthiobenz(cd)indole hydriodide | HCID 20150650 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178432904 | HCID 178432904 | 15.8% |
Reaction Steps
A mixture of 2.1 g of 3-(2-methyl-1H-imidazol-1-yl)propanamine, 5.0 g of 2-(methylthio)benz[cd]indole hydroiodide, 1.4 g of sodium acetate and 250 ml of ethanol was reacted as described in Example 13, giving 1.0 g of the desired product, mp 153°-155° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04728663 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-add3a2e67b7646968b466d125c5cf5d8 |
| Source note | uspto-grants-1988_03 |