HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 178419292, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 4-(Imidazole-1-yl)butylamine dihydrochloride | HCID 12803326 | — |
| Reactant | HCID 178527759 | HCID 178527759 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178419292 | HCID 178419292 | — |
Reaction Steps
A mixture 4.2 g of 4-(1H-imidazol-1-yl)butanamine dihydrochloride in 75 ml of ethanol was treated with 2.2 g of potassium hydroxide and stirred for 18 hours. A 5.2 g portion of 6-bromo-benz[cd]indole-2-thiol and 6.4 g of mercuric acetate were added and the reaction proceeded as described in Example 1, giving 3.7 g of the desired product, mp 145°-147° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04728663 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-98e348ef0de74a8ebf2a8e4a02b89482 |
| Source note | uspto-grants-1988_03 |