HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Amino-1,2-propanediol → HCID 178438306, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Amino-1,2-propanediol | HCID 73561 | — |
| Reactant | Allylbicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic anhydride | HCID 54206110 | — |
| Product | HCID 178438306 | HCID 178438306 | — |
Reaction Steps
102 g of allylbicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic anhydride are heated with 45.55 g of 2,3-dihydroxypropylamine to 200° C., and the pressure is lowered to 47 Pa. The yield is 138 g (96.5% of theory) of a highly viscous product having η80 =605 mPa.s and n25D =1.5380.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04728742 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-85b50b86da6d4f29be51c9410b7bb584 |
| Source note | uspto-grants-1988_03 |