HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Fluoro-2-nitrobenzene → HCID 14626470, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Fluoro-2-nitrobenzene | HCID 73895 | — |
| Reactant | Ammonium Acetate | HCID 517165 | — |
| Reactant | 1-(3,5-Difluoro-4-methoxyphenyl)methanamine | HCID 14626469 | — |
| Product | HCID 14626470 | HCID 14626470 | 100% |
Reaction Steps
A mixture of 2-fluoronitrobenzene (0.82 g, 5.8 mmole), 3,5-difluoro-4-methoxybenzylamine, (3.0 g, 17.3 mmole) and ammonium acetate (0.5 g) was reacted substantially as described in 1C above to yield 1.7 g, (100%) of the title compound as orange crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04728741 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-fbb3d18245cb4a8f9a85ff3579a82b51 |
| Source note | uspto-grants-1988_03 |