HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54286830, compound → HCID 20150807, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54286830 | HCID 54286830 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 20150807 | HCID 20150807 | — |
Reaction Steps
A solution of 30.6 g (0.14 mole) of 2-(1-cyanoprop-1-en-2-yl)-3-(2-methylprop-1-en-1-yl)-bicyclo[2.2.1]heptane in 100 ml of ethyl acetate was stirred together with 800 mg of 10% palladium on carbon at 90° C. in a hydrogen atmosphere under 90 bar, until the pressure remained constant for 5 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04728747 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-a43b5a18a1e342d6ade69e9028b706b7 |
| Source note | uspto-grants-1988_03 |