HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53779727, compound → HCID 20150803, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53779727 | HCID 53779727 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 20150803 | HCID 20150803 | — |
Reaction Steps
A solution of 60 g (0.22 mole) of 2-(1-ethoxycarbonylprop-1-en-2-yl)-3-(2-methylprop-1-en-1-yl)-bicyclo[2.2.1]heptane in 100 ml of ethyl acetate was stirred together with 1.6 g of palladium on alumina (0.5% strength) at 90° C. in a hydrogen atmosphere under 150 bar until the pressure remained constant for 5 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04728747 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-9c9238a1ce6943f7869bb45b531571e7 |
| Source note | uspto-grants-1988_03 |