HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54027108, compound → HCID 22002828, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54027108 | HCID 54027108 | — |
| Solvent | Ethanol ethylacetate | HCID 21584252 | — |
| Product | HCID 22002828 | HCID 22002828 | 90.9% |
Reaction Steps
Optically active p-benzyloxybenzoic acid p-(1-methylheptyloxy)phenyl ester (69.0 g, 0.16 mol) prepared above in (iv) was dissolved in a mixed solvent (2:1) (1,000 ml) of ethyl acetate-ethanol, followed by reducing it in the presence of 5% PdC (5.0 g) to obtain optically active p-hydroxybenzoic acid p-(1-methyl-heptyloxy)phenyl ester (49.8 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04729847 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-627908377dee44f0a504e66d9a4c5169 |
| Source note | uspto-grants-1988_03 |