Dipropylamine → HCID 20029851, compound

HRID 568872Notes

Reaction equation

[I:1][C:2]1[CH:10]=[CH:9][C:5]([C:6](Cl)=[O:7])=[CH:4][CH:3]=1.[CH2:11]([NH:14][CH2:15][CH2:16][CH3:17])[CH2:12][CH3:13]>>[CH2:11]([N:14]([CH2:15][CH2:16][CH3:17])[C:6](=[O:7])[C:5]1[CH:9]=[CH:10][C:2]([I:1])=[CH:3][CH:4]=1)[CH2:12][CH3:13]

Participants

Reactant 2

HCID 8902Dipropylamine

HCID 743734-Iodobenzoyl chloride

Product 1

HCID 20029851HCID 20029851, compound

Procedure

as an orange oil (11.51 g) t.l.c. (ER) Rf 0.48 was prepared from 4-iodobenzoyl chloride (10.0 g) and dipropylamine (4.10 g) according to the method of Intermediate 20.

Sources & evidence

ORD record: ord-bfb2a41ad71e464e9b45c5adb30c7e82
Source dataset: uspto-grants-1988_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04730008

Reaction notes

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