1,1-Dimethylhydrazine → HCID 13745533, compound

HRID 568942Notes

Reaction equation

HRID 568942 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([CH3:8])[C:3]=1[NH:9][C:10](=[O:15])[CH2:11][C:12](=[O:14])[CH3:13].CN(C)N>>[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([CH3:8])[C:3]=1[NH:9][C:10]([C:11]1[C:10](=[O:15])[CH:11]=[C:12]([CH3:13])[O:14][C:12]=1[CH3:13])=[O:15]

Participants

3

Reactant 2

HCID 59761,1-DimethylhydrazineHCID 20149863N-(2-Chloro-6-methylphenyl)-3-oxobutanamide

Product 1

HCID 13745533HCID 13745533, compoundYield 45%

Procedure

The title compound was prepared from N-(2-chloro-6-methylphenyl)-3-oxo-butanamide and N,N-dimethylhydrazine as the raw materials in a similar manner to the method described in Example 2. (Yield: 45%).

Sources & evidence

ORD record
ord-c96edd013a88486499b65a177675a277
Source dataset
uspto-grants-1988_03
Patent number
US04730061

Reaction notes

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