HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14097597, compound → HCID 131715469, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14097597 | HCID 14097597 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 131715469 | HCID 131715469 | 89% |
Reaction Steps
Tetraprotected amino acid (11) (118 mg, 0.24 mM) is refluxed in 6N HCl (20 ml) for 8 hours. After cooling the aqueous solution was washed with Et2O (3×25 ml) and evaporated to dryness in vacuo to yield the desired compound as a very hygroscopic white foam, 64 mg (89% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04730006 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-9d0a15e9cfb848f98dd9ad7c751b49d0 |
| Source note | uspto-grants-1988_03 |