HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20149456, compound → HCID 18611972, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20149456 | HCID 20149456 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 18611972 | HCID 18611972 | — |
Reaction Steps
2,6-di-t-butoxycarbonylamino-3,3-difluoro-1,7-heptanedioic acid (34 mg, 0.08 mmoles) is dissolved in dry ether saturated with HCl gas. After standing overnight and filtration, the title compound is obtained as a white solid (9 mg, 38%, RF: 0.4 (ethanol, conc. ammonia: 70/30, RF: 0.1 (butanol/acetic acid/water: 4/2/2)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04730006 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-6057e4b3b0d24b099b4a930858192e39 |
| Source note | uspto-grants-1988_03 |