Tributylstannane → HCID 54528940, compound

Participants

Reaction Steps

Heat a reaction mixture of 1.4 g (4.3 mmoles) of the title compound of Example 7 and 2.5 g (8.5 mmoles) of tri(n-butyl)tin hydride in 20 mL of toluene at reflux overnight. Evaporate to give a residue. Chromatograph the residue on silica gel, eluting with 1:1 (v/v) ethyl acetate:hexane to give the title compound as an oil, m/e 290.

Provenance & Evidence