HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 20148413, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | HCID 13315115 | HCID 13315115 | — |
| Solvent | Ethylene | HCID 6325 | — |
| Product | HCID 20148413 | HCID 20148413 | — |
Reaction Steps
150 mg of 6-ethoxycarbonyl-β-carboline are heated in 5 ml of ethylene gylcol with 2 ml of dimethylamine solution for 20 hours to 100° C. After cooling, it is placed on ice, extracted with ethyl acetate and the organic phase is dried, filtered and concentrated. 50 mg of 6-dimethylaminocarbonyl-β-carboline are obtained as oil after chromatography on silica gel with methylene chloride/ethanol=10:1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04731358 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-add9c74c1d444bdd96b0b82f2af42f84 |
| Source note | uspto-grants-1988_03 |