HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl bromide → HCID 53979939, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | HCID 13315139 | HCID 13315139 | — |
| Reactant | Diazabicycloundecane | HCID 57346892 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 53979939 | HCID 53979939 | — |
Reaction Steps
A solution of 0.28 g of 6-amino-β-carboline-4-carboxylic acid ethyl ester, 0.18 g of diazabicycloundecane and 0.26 g of allylbromide in 5 ml of ethanol is heated for 3 hours to 70° C. Then the solution is evaporated. The evaporation residue is extracted with ethyl acetate and water, the combined extracts are evaporated and chromatographed on silica gel with methylene chloride/methanol=5:1. Yield: 0.05 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04731358 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-725422a58abb4fc2a0e8a033cd31051b |
| Source note | uspto-grants-1988_03 |