HRID569044
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
0.5 g of 4-ethoxycarbonyl-3-(2-nitrovinyl)indole are heated under nitrogen for 45 minutes in the steam bath in 50 ml of formic acid with 1.5 g of 10% palladium-carbon. The palladium carbon is then filtered off, the filtrate evaporated, the evaporation residue [3-(2-aminoethyl)-4-ethoxycarbonyl indole] is then further reacted immediately.
WORKUP
后处理
- filtrationThe palladium carbon is then filtered off
- customthe filtrate evaporated
- customthe evaporation residue [3-(2-aminoethyl)-4-ethoxycarbonyl indole] is then further reacted immediately