HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Sulfamoylthieno[3,2-c]pyridine → 2-Sulfamoylthieno[3,2-c]pyridine-5-oxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Sulfamoylthieno[3,2-c]pyridine | HCID 20148568 | — |
| Reactant | Thieno[2,3-c]pyridine-2-sulfonamide | HCID 20148577 | — |
| Reactant | 2-Sulfamoylthieno[2,3-c]pyridine-6-oxide | HCID 20148592 | — |
| Product | 2-Sulfamoylthieno[3,2-c]pyridine-5-oxide | HCID 20148588 | — |
Reaction Steps
The title compound was prepared according to the procedure described for 2-sulfamoylthieno[2,3-c]pyridine-6-oxide (Example 3) except 2-sulfamoylthieno[3,2-c]pyridine was substituted for 2-sulfamoylthieno[2,3-c]pyridine. The title compound was obtained in 69% yield; m.p. 252°-254° C., after recrystallization from dimethyl sulfoxide/ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04731368 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-873c4810246b4ba380915ff87431ab50 |
| Source note | uspto-grants-1988_03 |