Water → HCID 23718750, compound

HRID 569122Notes

Reaction equation

HRID 569122 reaction equation
[Cl:1][C:2]1[C:13]([Cl:14])=[C:12]([C:15](=[O:20])[C:16](=[CH2:19])[CH2:17][CH3:18])[CH:11]=[CH:10][C:3]=1[O:4][CH2:5][CH2:6][C:7]([OH:9])=[O:8].O.C(=O)(O)[O-].[Na+:26]>>[Cl:1][C:2]1[C:13]([Cl:14])=[C:12]([C:15](=[O:20])[C:16](=[CH2:19])[CH2:17][CH3:18])[CH:11]=[CH:10][C:3]=1[O:4][CH2:5][CH2:6][C:7]([O-:9])=[O:8].[Na+:26]

Participants

4

Reactant 3

HCID 962WaterHCID 516892Sodium BicarbonateHCID 14099859HCID 14099859, compound

Product 1

HCID 23718750HCID 23718750, compound

Procedure

25 mg of 3-[2,3-dichloro-4-(2-methylenebutyryl)phenoxy]propionic acid is dissolved in 3.1 ml of 0.1N sodium bicarbonate and sufficient isotonic buffer to make a final volume of 10 ml. The water from all sources was pyrogen-free. The solution is sterilized by filtration.

Workup

  1. filtrationThe solution is sterilized by filtration

Sources & evidence

ORD record
ord-d537f7ab34ba493392d1fbde5a8e0d2e
Source dataset
uspto-grants-1988_03
Patent number
US04731381

Reaction notes

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