Water → HCID 23718751, compound

HRID 569124Notes

Reaction equation

HRID 569124 reaction equation
[Cl:1][C:2]1[C:15]([Cl:16])=[C:14]([C:17](=[O:23])[C:18](=[CH2:22])[CH2:19][CH2:20][CH3:21])[CH:13]=[CH:12][C:3]=1[O:4][C:5]1([C:9]([OH:11])=[O:10])[CH2:8][CH2:7][CH2:6]1.O.C(=O)(O)[O-].[Na+:29]>>[Cl:1][C:2]1[C:15]([Cl:16])=[C:14]([C:17](=[O:23])[C:18](=[CH2:22])[CH2:19][CH2:20][CH3:21])[CH:13]=[CH:12][C:3]=1[O:4][C:5]1([C:9]([O-:11])=[O:10])[CH2:8][CH2:7][CH2:6]1.[Na+:29]

Participants

4

Reactant 3

HCID 962WaterHCID 516892Sodium BicarbonateHCID 13958741HCID 13958741, compound

Product 1

HCID 23718751HCID 23718751, compound

Procedure

200 mg of 1-[2,3-dichloro-4-(2-methylenevaleryl)phenoxy]cyclobutane-1-carboxylic acid is dissolved in 31 ml of 0.1N sodium bicarbonate and sufficient isotonic buffer to make a final volume of 100 ml. The water from all sources was pyrogen free. The solution is sterilized by filtration.

Workup

  1. filtrationThe solution is sterilized by filtration

Sources & evidence

ORD record
ord-13b1ddf5c03b47e6a18dec3d9809cf43
Source dataset
uspto-grants-1988_03
Patent number
US04731381

Reaction notes

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