Water → Sodium 4-[2,3-dichloro-4-(2-methylenevaleryl)phenoxy]butyrate

HRID 569266Notes

Reaction equation

HRID 569266 reaction equation
[Cl:1][C:2]1[C:14]([Cl:15])=[C:13]([C:16](=[O:22])[C:17](=[CH2:21])[CH2:18][CH2:19][CH3:20])[CH:12]=[CH:11][C:3]=1[O:4][CH2:5][CH2:6][CH2:7][C:8]([OH:10])=[O:9].O.C(=O)(O)[O-].[Na+:28]>>[Cl:1][C:2]1[C:14]([Cl:15])=[C:13]([C:16](=[O:22])[C:17](=[CH2:21])[CH2:18][CH2:19][CH3:20])[CH:12]=[CH:11][C:3]=1[O:4][CH2:5][CH2:6][CH2:7][C:8]([O-:10])=[O:9].[Na+:28]

Participants

4

Reactant 3

HCID 962WaterHCID 516892Sodium BicarbonateHCID 139587354-[2,3-Dichloro-4-(2-methylenevaleryl)phenoxy]butyric acid

Product 1

HCID 23718749Sodium 4-[2,3-dichloro-4-(2-methylenevaleryl)phenoxy]butyrate

Procedure

250 mg of 4-[2,3-dichloro-4-(2-methylenevaleryl)phenoxy]butyric acid is dissolved in 62 ml of 0.1N sodium bicarbonate and sufficient isotonic buffer to make a final volume of 100 ml. The water from all sources was pyrogen free. The solution is sterilized by filtration.

Workup

  1. filtrationThe solution is sterilized by filtration

Sources & evidence

ORD record
ord-4fc150a7dcbe40b1a2b0a17373f29080
Source dataset
uspto-grants-1988_03
Patent number
US04731473

Reaction notes

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