Diethyl Ether → HCID 178419722, compound

Participants

Reaction Steps

The compound (3) (112 mg) obtained in Example 6 was dissolved in 1 ml of a 25% HBr/acetic acid solution and the mixture was stirred at room temperature for 30 minutes. To this reaction mixture was added ether to give a precipitate and supernatant was decanted twice. The residue was recrystallized from methanol-ether and collected by filtration. The product was washed with cold methanol-ether to give a white solid.

Provenance & Evidence