HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formic Acid → 3-(Phthalimido)-propyl formate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formic Acid | HCID 284 | — |
| Reactant | 2-(3-Hydroxypropyl)isoindoline-1,3-dione | HCID 70160 | — |
| Product | 3-(Phthalimido)-propyl formate | HCID 20147862 | — |
Reaction Steps
A mixture of 3-(phthalimido)-propanol (20.5 g) and formic acid (33 ml) was refluxed overnight and evaporated in vacuo to leave a yellow oil which crystallized from absolute ethanol to give colourless crystals with m.p. 68°-70° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04732998 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-106fdf697b954067947f319948b90715 |
| Source note | uspto-grants-1988_03 |