反应详情

A mixture of 3-(phthalimido)-propyl formate (17 g), phosphorus pentachloride (15.2 g) and alcoholfree chloroform was heated for 1 hour on the steam bath. After cooling and addition of ether, the crystalline product was isolated by filtration. M.p. 101°-103° C.

1. temperaturewas heated for 1 hour on the steam bath
2. temperatureAfter cooling
3. customthe crystalline product was isolated by filtration