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HRID569618

反应详情

EQUATION

反应方程式

HRID 569618 的结构方程式

REACTANTS

反应物

1
结构：CCOP(=O)(OCC)C(CC)(Oc1ccccc1)P(=O)(OCC)OCC
HCID53742288

未命名化合物

PRODUCTS

生成物

1
结构：CCC(Oc1ccccc1)(P(=O)(O)O)P(=O)(O)O
HCID20147886

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C[Si](C)(C)Br
溶剂HCID76113

Silane, bromotrimethyl-

C3H9BrSi

PROCEDURE

实验过程

A solution of tetraethyl (1-phenoxypropylidene)-bisphosphonate (2.1 g) in trimethyl bromosilane (8 ml) was kept at room temperature overnight, followed by evaporation in vacuo. The residue was stirred overnight in absolute ethanol. Evaporation in vacuo gave the desired compound.

WORKUP

后处理

  1. customfollowed by evaporation in vacuo
  2. customEvaporation in vacuo