HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 19921765, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Tetrahydro-1H-pyrrolizine-7a(5H)-carboxylic acid hydrochloride | HCID 44118652 | — |
| Product | HCID 19921765 | HCID 19921765 | 95.9% |
Reaction Steps
A mixture of pyrrolizidine-7a-carboxylic acid hydrochloride (24.6 g, 0.128 mol, prepared as described in Reference Example 2) and thionylchloride (280 ml, 3.89 mol) was stirred for 17 hours at 20° to 25° C. and the excess of thionylchloride was evaporated in vacuo to give 25.7g (95.9%) of the desired compound, as yellowish solids.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04734411 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-a8a6f945fcd14f9cbd87cd56c84cc2ed |
| Source note | uspto-grants-1988_03 |