HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → 2,1-Benzisothiazole-6-carboxaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | 2,1-Benzisothiazole-6-methanol | HCID 20146242 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2,1-Benzisothiazole-6-carboxaldehyde | HCID 20146260 | — |
Reaction Steps
1.65 g (10 mmol) of 10b are stirred analogously to Example 1b in 100 ml of CH2Cl2 and 30 ml of tetrahydrofuran with 5.5 g (63.4 mmol) of manganese(IV) oxide at room temperature overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04734407 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-e42d5361e2b241298e430638130ab6a6 |
| Source note | uspto-grants-1988_03 |