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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 569758Generated: October 30, 2026

HCID 22837354, compound → HCID 22837353, compound

https://huagongshe.com/reaction/569758

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 22837354HCID 22837354—
CatalystPalladiumHCID 23938—
ProductHCID 22837353HCID 22837353102.5%

Reaction Steps

Reduction of 1.9 g of t-butyl α-[3(S*)-azido-2-oxo-6(S*)-phenylperhydroazepin-1-yl]acetate (Isomer B) [prepared as described in Example 1(i)] with 5% w/w palladium-on-carbon in a similar manner to that described in Example 1(j) gave 1.8 g of the title compound as a gummy substance.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04734410
Source datasetuspto-grants-1988_03
ORD IDord-3fc2160b7ca34e649435599b767b2f34
Source noteuspto-grants-1988_03