HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanethiol → HCID 14698107, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanethiol | HCID 878 | — |
| Reactant | 5-(4-Fluorobenzoyl)-4-methyl-1,3-thiazol-2(3H)-one | HCID 14152258 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 14698107 | HCID 14698107 | — |
Reaction Steps
Gaseus methylmercaptan is added to a solution of 5-(4-fluorobenzoyl)-4-methyl-2(3H)-thiazolone (4.7 g) in ethanol (200 ml) to saturation. The mixture is heated at 120° C. in a sealed stainless steel container for 16 hours. After cooling to ambient temperature, the mixture is evaporated to dryness. The residue is recrystallized twice from ethanol to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04734422 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-fbab24ef11c248bdad4a086061127c68 |
| Source note | uspto-grants-1988_03 |