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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 569994Generated: October 31, 2026

HCID 13784124, compound → HCID 13784125, compound

https://huagongshe.com/reaction/569994

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 13784124HCID 13784124—
CatalystPalladiumHCID 23938—
SolventAcetic AcidHCID 176—
ProductHCID 13784125HCID 13784125—

Reaction Conditions

Temperature60 °C

Reaction Steps

While heating at 60° C. 1.6 g (5.18 mmol, Referential Example 42) of 2-(4-benzylpiperazino)-5-oxo-5,6-dihydro(7H)pyrrolo[3,4-d]pyrimidine, 0.16 g of 10% Pd-C and 30 ml of AcOH, H2 was bubbled. One hour later, Pd-C was filtered off and then the solvent was distilled off. The residue was suspended in a 10% aqueous NaHCO3 solution.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04734418
Source datasetuspto-grants-1988_03
ORD IDord-57770e55e1c34415ab250b86d61cf254
Source noteuspto-grants-1988_03