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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 569998Generated: October 30, 2026

Acetone → HCID 67906105, compound

https://huagongshe.com/reaction/569998

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetoneHCID 180—
Reactant4-Toluenesulfonyl chlorideHCID 7397—
ReactantPotassium HydroxideHCID 14797—
ReactantHCID 73187455HCID 73187455—
SolventWaterHCID 962—
ProductHCID 67906105HCID 67906105—

Reaction Steps

Added to a mixture of 30 ml of acetone, 2 g (5.35 mmol, Referential Example 49) of 2-(4-benzylpiperazino)-5,6,7,8-tetrahydro-5-hydroxyiminoquinazoline, and 1.6 g (8.4 mmol) of p-toluenesulfonyl chloride was a solution of 0.7 g (11 mmol) of KOH in 10 ml of water. The resultant mixture was stirred at 20° C. for 4 hours.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04734418
Source datasetuspto-grants-1988_03
ORD IDord-79fe383db0614223b01c6c5291078e2b
Source noteuspto-grants-1988_03