HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 67906105, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 73187455 | HCID 73187455 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 67906105 | HCID 67906105 | — |
Reaction Steps
Added to a mixture of 30 ml of acetone, 2 g (5.35 mmol, Referential Example 49) of 2-(4-benzylpiperazino)-5,6,7,8-tetrahydro-5-hydroxyiminoquinazoline, and 1.6 g (8.4 mmol) of p-toluenesulfonyl chloride was a solution of 0.7 g (11 mmol) of KOH in 10 ml of water. The resultant mixture was stirred at 20° C. for 4 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04734418 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-79fe383db0614223b01c6c5291078e2b |
| Source note | uspto-grants-1988_03 |