Pyrimidine → HCID 13769880, compound

Participants

Reaction Steps

Dissolved in 30 ml of ethanol was 1.2 g (3.07 mmol, Referential Example 79) of 2-(4-benzylpiperazino)-6-cyclohexyl-5-oxo-5,6-dihydro(7H)pyrrolo-[3,4-d]pyrimidine, followed by an addition of 0.16 g of 10% Pd-C. The pyrimidine derivative was hydrogenated at 60° C. After completion of the reaction, Pd-C was filtered off and ethanol was distilled off to obtain 0.92 g of the above-identified compound as crystals (yield: about 100%).

Provenance & Evidence