Ethyl trifluoroacetate → HCID 58587431, Verbindung

Beteiligte Stoffe

Reaktionsbedingungen

Reaktionsschritte

N-Methyl-1,3-diaminopropane (50 g, 0.56 mol) was dissolved in 200 mL acetonitrile followed by addition of ethyl trifluoroacetate (154 ml, 1.28 mol). The reaction mixture was stirred overnight at 85° C. The solvent was then removed in vacuo to yield the depicted product as a brown oil (101 g, 98.5%).

Herkunft & Nachweise