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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 570740Generated: October 30, 2026

Pyridinium chloride → HCID 86685396, compound

https://huagongshe.com/reaction/570740

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPyridinium chlorideHCID 10176127—
ReactantHCID 68015340HCID 68015340—
SolventDimethylformamideHCID 6228—
ProductHCID 86685396HCID 8668539656.3%

Reaction Conditions

Temperature120 °C

Reaction Steps

A mixture of 2-(ethylsulfanyl)-7-methoxy-3-[4-(2,2,2-trifluoroethoxy)phenyl]pteridin-4(3H)-one (92 mg), pyridine hydrochloride (640 mg) and N,N-dimethylformamide (3 ml) was stirred at 120° C. for 10 hr, and in the same manner as in Example 6, the title compound (50 mg) was obtained as a white powder.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09023858B2
Source datasetuspto-grants-2015_05
ORD IDord-56402f15807146eca4d5f3a24045af90
Source noteuspto-grants-2015_05