HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 86708897, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 131732812 | HCID 131732812 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86708897 | HCID 86708897 | — |
Reaction Steps
A solution of the product from Step A (0.19 g, 0.396 mmol) in TFA (1.5 mL) and DCM (1.5 mL) was stirred at rt for 1.5 h. Concentration by rotary evaporation was followed by dilution with DCM and additional evaporation to give the product as a TFA salt. LC/MS: C18H22F3N5O2: m/z 398.3 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09024017B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-90bd3bdc94cc46e6b8ac00cb34576264 |
| Source note | uspto-grants-2015_05 |