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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 571355Generated: October 31, 2026

Trifluoroacetic acid → HCID 86708897, compound

https://huagongshe.com/reaction/571355

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 131732812HCID 131732812—
SolventDichloromethaneHCID 6344—
ProductHCID 86708897HCID 86708897—

Reaction Steps

A solution of the product from Step A (0.19 g, 0.396 mmol) in TFA (1.5 mL) and DCM (1.5 mL) was stirred at rt for 1.5 h. Concentration by rotary evaporation was followed by dilution with DCM and additional evaporation to give the product as a TFA salt. LC/MS: C18H22F3N5O2: m/z 398.3 (M+H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09024017B2
Source datasetuspto-grants-2015_05
ORD IDord-90bd3bdc94cc46e6b8ac00cb34576264
Source noteuspto-grants-2015_05