HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 131732814, compound → HCID 86708905, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 131732814 | HCID 131732814 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 86708905 | HCID 86708905 | — |
Reaction Steps
A solution of the product from Step A (0.08 g, 0.156 mmol) in TFA (1.5 mL) and DCM (1.5 mL) was stirred at rt for 1.5 h. The volatile organic compounds were removed by evaporation, and the residue was diluted with DCM and evaporated again to give the product as a TFA salt. LC/MS: C19H24F3N5O2: m/z 412.5 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09024017B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-269ace6d04bd480aa1f2a93b02361da2 |
| Source note | uspto-grants-2015_05 |