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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 571358Generated: November 3, 2026

HCID 131732814, compound → HCID 86708905, compound

https://huagongshe.com/reaction/571358

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 131732814HCID 131732814—
SolventDichloromethaneHCID 6344—
SolventTrifluoroacetic acidHCID 6422—
ProductHCID 86708905HCID 86708905—

Reaction Steps

A solution of the product from Step A (0.08 g, 0.156 mmol) in TFA (1.5 mL) and DCM (1.5 mL) was stirred at rt for 1.5 h. The volatile organic compounds were removed by evaporation, and the residue was diluted with DCM and evaporated again to give the product as a TFA salt. LC/MS: C19H24F3N5O2: m/z 412.5 (M+H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09024017B2
Source datasetuspto-grants-2015_05
ORD IDord-269ace6d04bd480aa1f2a93b02361da2
Source noteuspto-grants-2015_05