HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → (S)-2-(methylthio)-1-phenylethanaminium chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 89535947 | HCID 89535947 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | (S)-2-(methylthio)-1-phenylethanaminium chloride | HCID 89524515 | 95% |
Reaction Steps
(S)-tert-butyl (2-(methylthio)-1-phenylethyl)carbamate (380 mg, 1.421 mmol) was dissolved in HCl (1066 μl, 4.26 mmol) in dioxane and allowed to stir for 30 minutes at rt. The solvents were removed in vacuo to provide (S)-2-(methylthio)-1-phenylethanaminium chloride (275 mg, 1.350 mmol, 95% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09023865B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-4580b21485cc4493be5dc0375cb8b6be |
| Source note | uspto-grants-2015_05 |