HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propanethioamide → HCID 86697863, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propanethioamide | HCID 2760628 | — |
| Reactant | 5-Bromoazepan-4-one hydrobromide | HCID 22620766 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86697863 | HCID 86697863 | — |
Reaction Steps
0.40 g (1.47 mmol) 5-bromo-azepan-4-one hydrobromide, 0.13 g (1.47 mmol) thiopropionamide and 3 mL ethanol were stirred under reflux for 3 hours. The reaction was allowed to cool to RT and was filtered. The filtrate was concentrated to dryness and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09029360B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-c956829b3f564bf7ae02c6c68cda58b7 |
| Source note | uspto-grants-2015_05 |